Adhesion Measurement of Films and Coatings, Volume 2 by Kash L. Mittal

By Kash L. Mittal

This booklet files the lawsuits of the second one foreign Symposium on Adhesion size of movies and Coatings, held in Newark, NJ, October 25-27, 1999. This quantity includes 20 papers, that have all been carefully peer reviewed and certainly changed prior to inclusion. the subjects comprise: dimension and research of interface adhesion; relative adhesion size for skinny movie constructions; adhesion checking out of not easy coatings through a number of ideas; dimension of interfacial fracture power in multifilm purposes; laser caused decohesion spectroscopy (LIDS) for measuring adhesion; pulsed laser approach for evaluation of adhesion; blade adhesion try out; JKR adhesion try out; coefficient of thermal enlargement size; and residual stresses in diamond movies.

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One may not even know about them all, unless a very detailed analysis of the testing process is done. This detailed analysis does not only include the XPS and SEM analyses discussed here, but must include the calorimetric evaluation of the test, as well as acoustic and fractoemission detections. It is unlikely that one would go to such lengths in a practical situation to assure that all energy-dissipating processes were being taken into account in order to calculate the fundamental adhesion. As it has been stated before [ 11, for practical situations in the manufacturing environment, where quick response in problem solving is financially essential, a way has to be found where a simple straightforward adhesion testing can be used with reliable results.

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Changes in the sample preparation for the MELT testing to control the delamination shape have been suggested. One may consider an etchback process to create a uniform precrack by etching into the film from the edges. Shaffer [60] has used this approach with polymer/metal interfaces. He chose FeC13 as the etchant to create the precrack. Cyclotene and Ultradel (Dow Chemical) interfaces with AlCu and Cu were extremely sensitive to the FeC13 etchant. Shaffer showed that the calculated I

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